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27977 - Polymer Science Fundamentals L

Academic Year 2012/2013

Teacher Daniele Caretti
Number of credits 5
SSD CHIM/05
Teaching Mode Traditional lectures
Lingua Italian
Versione italiana

Learning outcomes

The students will achieve basic knowledge of  polymer science and will acquire the skills for synthesis and characterization of polymeric products. 


Course contents

Introduction to macromolecular chemistry 
Homopolymers and copolymers, configuration and stereoregularity, macromolecules conformations, polymerization process, molecular weight and molecular weight distribution, structure - properties correlations  
   
Step growth polymerization 
Step growth reactions, experimental parameters effects on step growth polymerization , examples of step growth polymerization  
   
Chain polymerization 
Radical polymerization, radical polymerization techniques, cationic polymerization, anionic polymerization, Ziegler Natta polymerization.  
   
Copolymers 
Copolymers classification, reactivity ratio definitions and their effect on copolymer composition, copolymers synthesis  
   
Polymer reactions 
Functionalization of polymers, industrial examples of polymer reactions, polymer crosslinking  
   
Polymer crystallinity 
Crystallization from polymer melt, crystallization degree and its experimental determination, polymer crystallization kinetic  
   
Molecular weight 
Determination of polymer molecular weight by colligative properties, viscosimetry, size exclusion chromatography, other methods for molecular weight determination  
   
Glass transition temperature 
Definition of glass transition, internal and external factors influencing glass transition, glass transition determination  
       
Polymeric materials degradation 
Thermal and chemical degradation of polymers, depolymerization techniques, polymer recycle, compatibilization, thermovalorization


In laboratory some experiences related to the Polymer Science will be carried out:

  • Synthesis and characterization of polymers copolymers 
  • Polymeric materials identification
  • Determination of phisico – chemical parameters of polymers

Readings/Bibliography

- Associazione Italiana di Scienza e Tecnologia delle Macromolecole,Fondamenti di Scienza dei Polimeri , Pacini editore (1998)


- S. Bruckner, G. Allegra, M. Pegoraro, F.P. La Mantia, Scienza e Tecnologia dei Materiali Polimerici , Edises editore (2001)


Teaching methods

Lectures and  exercises carried out in the classroom. In the laboratory some experimental activity will be done

Assessment methods

Assessment of the course will be via an oral exam.  

Teaching tools

Lectures and  exercises carried out in the classroom are integrated with practical activities in the chemical laboratory.  

Language of instruction

Italian

Office hours

See the Faculty member's website